Download e-book for iPad: Clean Technology for the Manufacture of Specialty Chemicals by W Hoyle, Mike Lancaster

By W Hoyle, Mike Lancaster

ISBN-10: 0854048855

ISBN-13: 9780854048854

Generating huge amounts of waste isn't just environmentally unacceptable, it's also no longer potential in monetary phrases. The chemical undefined, really the speciality and prescribed drugs sectors, is changing into more and more conscious of the benefits linked to fresh know-how, relatively when it comes to aggressive virtue and environmental merits. Bringing jointly an realizing of the strategies and values of fresh expertise through the use of case reviews from a few prime eu nations, this publication presents an perception into topics resembling catalysis; procedure intensification; and the way to degree the "green" worth of a technique. It additionally highlights the position performed through either the chemical and chemical engineering disciplines within the improvement of cleanser strategies. fresh expertise for the Manufacture of Speciality chemical compounds will end up helpful examining for technique improvement chemists and engineers, rather these within the specialities and prescribed drugs sectors, and also will be an incredible resource of educating fabric for the starting to be variety of fresh expertise chemistry classes.

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3 4 The anticipated large-scale costs and availability of TDA-1 prompted us to investigate the role of the catalyst system in order to allow us to reduce the molar ratio. 8 to <3 by the completion of the reaction. We attribute the pH change to formation of small quantities of sulphonic acid derivatives. The observation of pH change was puzzling in two ways; how did the pH drift effect the catalyst system and what was the optimum pH for the reaction. It is known that molybdate anions undergo oligomerization.

H. M. R. Cramers, A. A. C. M. Beenackers and L. L. van Dierendonck, Polytech. , 1993,48 (2), 42. 10. P. H. M. R. Cramers, L. Smit, G. M. Leuteritz, L. L. van Dierendonck and A. A. C. M. Beenackers, Chem. Eng. , 1993,53 (l), 67. 46 Clean Technology for the Manufacture of Speciality Chemicals 11. P. H. M. R. Cramers, R. F. Duveen and L. L van Dierendonck, “Process Intensification with Buss loop reactors”, Proc. Eur. Symp. on Catalysis in Multiphase Reactors, 1994. 12. D. Nardin and P. H. M. R. Cramers, Spec.

Because microreactors are just getting off the age of childhood there is only limited information available for setting up a process design for a given reaction system. l~ In the model system considered here, advantage can be taken of the enhanced heat exchanging capacity. For instance a combination of a microreactor together with a plug flow reactor (static mixer) might be an attractive set-up. g. 90% as well as removing the corresponding amount of reaction heat. The plug flow reactor could serve for finishing off the reaction to a complete conversion.

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Clean Technology for the Manufacture of Specialty Chemicals by W Hoyle, Mike Lancaster

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